黄金桂茶叶精油固香缓释研究

doi:10.13305/j.cnki.jts.2016.04.005

Abstract

Abstract: An optimized and improved SDE method was carried out to get tea essential oil of high fidelity and the optimum condition was 2 h extraction of 25 g tea by continuous hot flowing steam. The effects of fixatives (diethyl phthalate, benzyl benzoate and vanillin) on this tea essential oil and their roles on the performance of aroma slow-release in tea essential oil were also studied by GC/MS and olfactory evaluation. The results showed that the persistence of fragrance was improved by all 3 fixatives. Among these, tea essential oil with diethyl phthalate showed highest fidelity of original odor type, indicating diethyl phthalate could be applied to manufacture tea aroma standard reference. Vanillin showed the best performance for aroma slow-release but the lowest fidelity. Benzyl benzoate had excellent coordinate ability and showed good performance for both fidelity and persistence which can be applied to develop tea fragrances. This study provided new ideas for fidelity and slow-release of tea essential oil. Meanwhile, the theoretical and practical foundation was established for hypostatization of tea olfactory term and innovation of tea fragrance and other field of tea industry.

Key words: fixative, tea essential oil, aroma, slow-release, fidelity

CLC Number:

TS272
Q946.8

LIU Wanqiong1, ZHANG Yingbin2, GONG Shuying1*, CHEN Ping1, FAN Fangyuan1, YANG Mengxuan1, GU Zhaoqi1. Effects of Different Fixatives on Fidelity and Slow-release of Huangjingui Tea Essential Oil Aroma[J]. Journal of Tea Science, 2016, 36(4): 372-378.

References

[1] 中华人民共和国国家质量技术监督检验检疫局, 中国国家标准化管理委员会. GB/T 23776—2009 茶叶感官审评方法[S]. 北京:中国标准出版社, 2009.
[2] 施梦南, 龚淑英. 茶叶香气研究进展[J]. 茶叶, 2012, 38(1):19-23.
[3] 袁海波, 尹军峰, 叶国柱, 等. 茶叶香型及特征物质研究进展[J]. 中国茶叶, 2009, 31(8): 14-15.
[4] 都业俭. 植物芳香性成分保真高效提取研究[D]. 重庆: 重庆大学, 2011.
[5] 郑鹏程, 方世辉. 茶叶香精油的提取制备方法[J]. 中国茶叶加工, 2008(2): 39-41.
[6] 朱旗, 施兆鹏, 任春梅. 绿茶香气不同提取方法的研究[J]. 茶叶科学, 2001, 21(1): 38-43.
[7] M Shimoda, H Shigematsu, H Shiratsuchi, et al.Comparison of the odor concentrates by SDE and adsorptive column method from green tea infusion[J]. Journal of Agricultural and Food Chemistry, 1995, 43(6): 1616-1620.
[8] 施梦南. 基于一种新SDE法对茶叶香气的分析研究[D]. 杭州: 浙江大学, 2014.
[9] 葛艳蕊. 缓释型香精微胶囊的研制[D]. 北京: 北京化工大学, 2003.
[10] 张承曾, 汪清如. 日用调香术[M]. 北京: 轻工业出版社, 1989.
[11] 黄龙珠, 张席席, 朱腾高, 等. 香水中邻苯二甲酸二乙酯的直接质谱分析研究[J]. 质谱学报, 2014, 35(06): 550-554.
[12] 陈玲, 李剑政, 杨文彬, 等. “清水芙蓉”香水的香气成分分析[J]. 分析测试学报, 2005, 24(9): 214-216.
[13] 原玲芳, 敖明章, 金文闻, 等. 香兰素延缓桂花精油香气释放的研究[J]. 食品科学, 2013, 34(19): 73-75.
[14] 唐德松, 龚淑英. 可控温度的同时萃取装置及使用方法: CN201310047211[P].2014-08-06
[15] 中华人民共华国卫生部. GB 2760—2011食品添加剂使用标准——附录B食品用香料使用规定[S]. 北京: 中国标准出版社, 2011.
[16] 曹婷婷. 机采岩毛茶精制工艺及烘焙与香气品质的研究[D]. 杭州: 浙江大学, 2015.
[17] Teixeira M A, Rodríguez O, Mata V G, et al.The diffusion of perfume mixtures and odor performance[J]. Chemical Engineering Science, 2009, 64(11): 2570-2589.
[18] W Sturm.合成香料的香气持久性与定香[J]. 上海日用化工, 1977(1): 69-83.
[19] 林翔云. 定香机理及定香基的配制[J]. 香精香料化妆品, 2011, 2(1): 47-51.
[20] 林翔云, 王丽萍, 林君如, 等. 自然界气味关系图[J]. 香精香料化妆品, 2015, 2(1): 66-73.
[21] 林翔云. 调香术[M]. 北京: 化学工业出版社, 2008.
[22] Clark GS. A Profile: An Aroma Chemical [J]. Perfumer & flavorist, 1990, 15: 45- 46, 50, 52-54.
[23] 余丹丹, 邵兴锋, 许凤, 等. 茶树精油在果实采后保鲜中的作用及其机制研究进展[J]. 果树学报, 2014(2): 313-319.

Effects of Different Fixatives on Fidelity and Slow-release of Huangjingui Tea Essential Oil Aroma

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